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標題: Electrochemical Dehydrogenative Phosphorylation of Thiols
作者: Chung-Yen Li 
Chin-Fa Lee 
Daggula Mallikarjuna Reddy 
Yi-Xuan Li 
You-Chen Liu 
We report herein a new approach for the synthesis of organothiophosphates from phosphonates and thiols through electrochemical reaction. The reactions were conducted without the addition of oxidant, transition-metal base, or base at room temperature. This system has a good substrate scope and functional group tolerance. Aryl and alkyl thiols worked well with phosphonates to afford the corresponding organothiophosphates in good yields.
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