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標題: Analysis of volatile compounds emitted from fresh Syringa oblata flowers in different florescence by headspace solid-phase microextraction-gas chromatography-mass spectrometry
作者: Li, Z.G.
Lee, M.R.
Shen, D.L.
關鍵字: Syringa oblata;solid-phase microextraction (SPME);gas;chromatography-mass spectrometry (GC-MS);volatile compounds;sample preparation;constituents;scent;spme;tool
Project: Analytica Chimica Acta
期刊/報告no:: Analytica Chimica Acta, Volume 576, Issue 1, Page(s) 43-49.
In this study, a simple and solvent-free method was developed for determination of the volatile compounds from fresh flowers of Syringa oblata using headspace solid-phase microextraction and gas chromatography-mass spectrometry. The SPME parameters were studied, the optimum conditions of a 65 mu m polydimethylsiloxan/divinylbenezene (PDMS/DVB), extraction temperature of 25 degrees C and extraction time of 30 min were obtained and applied to extraction of the volatile compounds emitted from fresh flowers of S. oblata. The volatile compounds released from fresh flowers of S. oblata were separated and identified by GC-MS. Lilac aldehyde A, lilac aldehyde B, lilac aldehyde C, lilac aldehyde D, lilac alcohol A, lilac alcohol B, lilac alcohol C, lilac alcohol D, a-pinene, sabinene, P-pinene, myrcene, D-limonene, eucalyptol, cis-ocimene, benzaldehyde, terpinolene. linalool, benzene acetaldehyde, alpha-terpineol, p-methoxyanisole, p-anisaldehyde, (ZE)-alpha-famesene and (E,E)-alpha-famesene were the most abundant volatiles released from fresh flowers of S. oblata var. alba. The relative contents of main volatile fragrance were found to be different in emissions from two varieties of S. oblata flowers (white or purple in color). The four isomers of lilac alcohol and four isomer lilac aldehyde were the characteristic components of the scent of fresh flowers of S. oblata. The main volatile fragrance from fresh flowers of S. oblata var. alba in different florescence ((A) flower buds; (B) at the early stage of flower blooming; (C) during the flower blooming; (D) at the end of flower blooming; (E) senescence) were studied in this paper. The results demonstrated that headspace SPME-GC-MS is a simple, rapid and solvent-free method suitable for analysis of volatile compounds en-fitted from fresh flowers of S. oblata in different florescence. (c) 2006 Elsevier B.V. All rights reserved.
ISSN: 0003-2670
DOI: 10.1016/j.aca.2006.01.074
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