Please use this identifier to cite or link to this item: http://hdl.handle.net/11455/3711
DC FieldValueLanguage
dc.contributor張新福zh_TW
dc.contributor王國華zh_TW
dc.contributor.advisor鄭紀民zh_TW
dc.contributor.author劉威成zh_TW
dc.contributor.authorLiu, Wei-Chengen_US
dc.contributor.other中興大學zh_TW
dc.date2009zh_TW
dc.date.accessioned2014-06-06T05:32:32Z-
dc.date.available2014-06-06T05:32:32Z-
dc.identifierU0005-2907200815494200zh_TW
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dc.identifier.urihttp://hdl.handle.net/11455/3711-
dc.description.abstract本研究利用醇還原法製備奈米介金屬鎳/鎂合金,作為成長奈米碳管所用之觸媒,以化學氣相沉積法成長奈米碳管,並將奈米銀粒子擔持到酸處理後之奈米碳管表面,利用不同之酸處理方法及不同之擔持量,以TGA、FT-IR、XRD及TEM進行特性分析,探討其奈米銀粒子之粒徑大小及分布,並將擔持奈米銀粒子之奈米碳管對大腸桿菌進行抗菌測試。 研究結果顯示,奈米銀粒子其粒徑大小隨著前驅物添加量的增加,平均粒徑亦有漸增趨勢,以硝酸法處理過的奈米碳管,可在其表面得到分散良好的奈米銀粒子,在樣品濃度5zh_TW
dc.description.abstractThis study will use the chemical reduction method such as polyolprocess to prepare the nano intermetallic alloys catalyst (NiMg) and synthesize carbon nanotube with the Chemical Vapor Deposition method. Then using of strong oxidants, such as HNO3 and HCl, is applied to oxidize CNTs to form carboxylic acid group and hydroxyl group. The silver nanoparticles will be deposited onto the modified CNTs. The physical properties and structural information were characterized by TGA, XRD, TEM and FT-IR. Finally, the (Ag/CNT) efficiency studied using E. coli. The nanoscale and well-dispersed a silver nanoparticles on the CNT can be obtained due to the carbon nanotubes with HNO3 treatment. In addition, the sample in the density 5 mg/ml has close on 100% efficiency and the (Ag/CNT) load in 10 wt% possesses the highest efficiency of E. coli test. The results of TEM, we prove the nano-particles and dispersity can enhance the efficiency of the (Ag/CNT) in E coli test.en_US
dc.description.tableofcontents中文摘要---------------------------------------------------i 英文摘要--------------------------------------------------ii 目錄-----------------------------------------------------iii 圖目錄-----------------------------------------------------v 表目錄---------------------------------------------------vii 第一章 緒論------------------------------------------------1 第二章 文獻回顧--------------------------------------------3 2-1 奈米碳管----------------------------------------3 2-1-1 奈米碳管發展簡介----------------------------3 2-1-2 奈米碳管的結構------------------------------4 2-1-3 奈米碳管之特性------------------------------8 2-1-4 奈米碳管的酸處理---------------------------12 2-1-5 奈米碳管應用-------------------------------14 2-2 奈米抗菌材料-----------------------------------18 2-2-1 微生物簡介---------------------------------18 2-2-2 抗菌材料之種類-----------------------------22 2-2-3 無機奈米抗菌材料及抗菌原理-----------------27 2-2-4 抗菌材料之應用-----------------------------29 第三章 實驗設備與研究方法---------------------------------32 3-1 實驗藥品---------------------------------------32 3-2 實驗儀器---------------------------------------33 3-3 研究方法---------------------------------------34 3-3-1 奈米介金屬觸媒製備-------------------------34 3-3-2 奈米碳管合成-------------------------------34 3-3-3 奈米碳管純化-------------------------------36 3-3-4 奈米銀擔持於奈米碳管之製備-----------------36 3-3-5 奈米銀擔持於奈米碳管之特性分析-------------37 3-3-6 奈米銀擔持於奈米碳管之抗菌實驗-------------41 第四章 實驗結果與討論-------------------------------------43 4-1 奈米碳管的製備分析-----------------------------43 4-2 奈米碳管的酸處理分析---------------------------47 4-2-1 奈米碳管純化之分析-------------------------48 4-2-2 奈米碳管表面的官能基化之分析---------------52 4-3 奈米銀粒子擔持於奈米碳管之製備及分析-----------54 4-3-1 熱重損失分析-------------------------------55 4-3-2 X光繞射儀分析------------------------------58 4-3-3 穿透式電子顯微鏡分析-----------------------60 4-4 奈米銀擔持於奈米碳管之抗菌分析-----------------67 4-4-1 未擔持奈米銀粒子之奈米碳管對抗菌性之影響---67 4-4-2 不同酸處理之奈米碳管擔持奈米銀粒子對抗菌性的- 影響---------------------------------------69 4-4-3硝酸處理之奈米碳管擔持奈米銀粒子之擔持量對抗- 菌性的影響----------------------------------70 4-4-4鹽酸處理之奈米碳管擔持奈米銀粒子之擔持量對抗-- 菌性的影響----------------------------------71 第五章 結論-----------------------------------------------78 參考文獻--------------------------------------------------79zh_TW
dc.language.isoen_USzh_TW
dc.publisher化學工程學系所zh_TW
dc.relation.urihttp://www.airitilibrary.com/Publication/alDetailedMesh1?DocID=U0005-2907200815494200en_US
dc.subjectcarbon nanotubesen_US
dc.subject奈米碳管zh_TW
dc.subjectsilver nanoparticlesen_US
dc.subjectantibacterial.en_US
dc.subject奈米銀zh_TW
dc.subject抗菌性zh_TW
dc.title奈米銀粒子擔持於奈米碳管之製備與抗菌性研究zh_TW
dc.titleSynthesis and Antibacterial Activities of Silver Nanoparticles Supported on Carbon Nanotubesen_US
dc.typeThesis and Dissertationzh_TW
item.languageiso639-1en_US-
item.openairetypeThesis and Dissertation-
item.cerifentitytypePublications-
item.grantfulltextnone-
item.fulltextno fulltext-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
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