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標題: Adsorption separation of terpene lactones from Ginkgo biloba L. extract using glass fiber membranes modified with octadecyltrichlorosilane
作者: Su, I.F.
Chen, L.J.
Suen, S.Y.
關鍵字: glass fiber membrane;octadecyltrichlorosilane;adsorption separation;terpene lactones;Ginkgo biloba L. extract;performance liquid-chromatography;hydrophobic interaction;affinity;membrane;protein separation;porous membrane;small molecules;leaf;extracts;purification;monolayers;leaves
Project: Journal of Separation Science
期刊/報告no:: Journal of Separation Science, Volume 28, Issue 11, Page(s) 1211-1220.
In this study porous glass fiber membranes were modified by reaction with octadecyltrichlorosilane to form C18 hydrophobic membranes. The contact angle and the CH2 vibration bands at 2855 and 2920 cm(-1) found by FTIR measurements verified the successful immobilization of C18 groups on the glass fiber membranes. The resulting C18 hydrophobic membranes were used to adsorb terpene lactones from crude Ginkgo biloba L. extracts. In batch adsorption processes, the modified C18 membranes exhibited a better adsorption performance than commercial C18 solid phase extraction adsorbents. Different desorption solvents were tested and ethyl acetate was found to preferentially desorb terpene lactones from the modified C18 membranes. In flow adsorption experiments at 1 mL/min, terpene lactone contents higher than 6 wt% (the standardized content) could be achieved in the elution step using ethyl acetate.
ISSN: 1615-9306
DOI: 10.1002/jssc.200400017
Appears in Collections:化學工程學系所

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